Phenyl 2,3,4-tri-O-benzyl-1-thio-α-D-mannopyranoside monohydrate

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Phenyl 2,3,4-tri-O-benzyl-1-thio-α-d-mannopyran­oside monohydrate

In the title compound, C(33)H(34)O(5)S·H(2)O, the mannopyran-oside ring adopts a chair conformation with the 2-α-thio-phenyl group occupying an axial position. One of the pendant benzyl groups is disordered over two sets of sites in a 0.5:0.5 ratio. In the crystal, the water mol-ecule makes two O-H⋯O hydrogen bonds to an adjacent sugar mol-ecule with the O atoms of the primary alcohol and ether...

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Phenyl 2,3-O-isopropyl­idene-1-thio-α-d-rhamnopyran­oside

In the title compound, C(15)H(20)O(4)S, a dioxolane ring is fused to the pyran ring of the sugar which carries a thio-phenyl substituent on the anomeric C atom. The dioxolane ring adopts an envelope conformation and the pyran ring system a distorted (4)C(1) chair. The structure is stabilized by O-H⋯O hydrogen bonds, forming centrosymmetric dimers that generate an R(2) (2)(10) ring motif. Additi...

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1-O-Acetyl-3,4,6-tri-O-benzyl-2-C-bromo­methyl-2-de­oxy-α-d-glucopyran­ose

In the title compound, C30H33BrO6, the pyran-ose ring adopts a chair conformation. Two of the O-benzyl phenyl rings lie almost perpendicular to C/C/C/O plane formed by the ring atoms not attached to these O-benzyl phenyl rings, and form dihedral angles of 85.1 (2) and 64.6 (2)°, while the third O-benzyl phenyl ring is twisted so that it makes a dihedral angle 34.9 (2)° to this C/C/C/O plane. Th...

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Phenyl 4,6-di-O-acetyl-2,3-dide­oxy-1-thio-α-d-erythro-hex-2-enopyran­oside

The pyranosyl ring in the title compound, C(16)H(18)O(5)S, adopts an envelope conformation, with the acetyl groups in equatorial positions. In the crystal, weak C-H⋯O inter-actions link the molecules into chains.

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p-Tolyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzyl­idene-1-thio-α-l-idopyran­oside

The title compound, C(34)H(32)O(6)S, is an ido-configured thio-glycoside building block for heparan sulfate fragments. It contains disordered tolyl and O-benzyl groups with occupancy ratios of 0.539 (13):0.461 (13) and 0.613 (13):0.387 (13), respectively, as determined from a weakly diffracting crystal. The fused rings adopt chair conformations with the mol-ecules packing into a three-dimension...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2010

ISSN: 1600-5368

DOI: 10.1107/s1600536810019604